| 論文名 |
Optimisation methodology in the chiral and achiral separation in electrokinetic chromatography in the case of a multicomponent sample of dansyl amino acids. |
| 著者 |
Alessandro Giuffrida
Marianna Messina
Annalinda Contino
Vincenzo Cucinotta
|
| キーワード |
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| 出版年月 |
1970年1月 |
| 発表先 |
J Pharm Biomed Anal. 2013 Nov;85:55-60. |
| WEBサイト |
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| 論文概要(和文) |
ダンシルアミノ酸の多成分サンプルの場合の界面動電クロマトグラフィーにおけるキラルおよびアキラル分離の最適化方法論。 |
| 論文概要(英文) |
Two different chiral selectors synthesised in our laboratory were used to test the possibility of separation for a sample consisting of ten different enantiomeric pairs of dansyl-derivatives of α-amino acids in electrokinetic chromatography. It was possible to observe all the peaks, though only partly resolved, due to the twenty analytes through an accurate strategy of choice of the experimental conditions. As a part of this strategy, a procedure of identification of the single peaks in the electropherograms called LACI (lastly added component identification) has been developed. |